Cover
Vol. 1 No. 1 (2025): ETES

Published: December 31, 2025

Pages: 31-36

Research Article

Al₂O₃ Nano and Micro Films Deposited using PLD on Stainless Steel Substrates for Medical Applications

Abstract

In this study, we deposited the Al2O3 nanostructure on 304 stainless steel using PLD technique. The stainless-steel specimens were successfully coated with Al2O3 nanostructure, and surface morphology was examined using an optical microscope. The findings confirmed the nanostructured nature of the films. Tafel curve analysis was used to determine the polarization of the sample before being subjected to laser shock penning treatment. Additional tests were then carried out on the samples following pulse laser deposition.

References

  1. D. A. Mohammed, M. A. Fakhri, and A. Kadhim, "Reduction the Corrosion Rate of 304 Stainless Steel using Pulsed Laser Shock Penning Method," IOP Conference Series: Materials Science and Engineering, vol. 454, no. 1, p. 012162, 2018/12/01 2018, doi: 10.1088/1757-899X/454/1/012162.
  2. J. Grum, "Comparison of different techniques of laser surface hardening," Journal of Achievements in Materials and Manufacturing Engineering, vol. 24, no. 1, pp. 17-25, 2007.
  3. Y. Xiong, T. He, Z. Guo, H. He, F. Ren, and A. A. Volinsky, "Effects of laser shock processing on surface microstructure and mechanical properties of ultrafine-grained high carbon steel," Materials Science and Engineering: A, vol. 570, no. May, pp. 82-86, 2013/05/15/ 2013, doi: https://doi.org/10.1016/j.msea.2013.01.068.
  4. M. A. Fakhri, S. F. H. Alhasan, N. H. Numan, J. M. Taha, and F. G. Khalid, "Effects of laser wavelength on some of physical properties of Al2O3 nano films for optoelectronic device," AIP Conference Proceedings, vol. 2213, no. 1, p. 020227, 2020, doi: https://doi.org/10.1063/5.0000183.
  5. S. S. Kubsad, B. Siddeswarappa, and B. Sridhar, "Effect of shock waves on wear behavior of few metallic materials," International Journal of Engineering Science and Technology (IJEST), vol. 4, no. 5, pp. 2425-2431, 2012.
  6. A. A. Al-Amiery, F. A. Binti Kassim, A. A. H. Kadhum, and A. B. Mohamad, "Synthesis and characterization of a novel eco-friendly corrosion inhibition for mild steel in 1 M hydrochloric acid," Scientific Reports, vol. 6, no. 1, p. 19890, 2016/01/22 2016, doi: https://doi.org/10.1038/srep19890.
  7. I. A. Abbas and K. H. Al-Mayalee, "Structural and Optical Properties of Al2O3 Nanostructures Prepared by Hot Water Treatment Method," Revue des Composites et des Materiaux Avances, vol. 34, no. 4, pp. 527-532, 2024, doi: https://doi.org/10.18280/rcma.340414.
  8. M. H. Ayman et al., "Hardness Optimization Using Takeuchi and ANOVA Method for Al2O3 Nano-Coating by PLD Systems," International Journal of Nanoelectronics and Materials (IJNeaM), vol. 18, no. June, pp. 269-279, 07/23 2025, doi: https://doi.org/10.58915/ijneam.v18iJune.2363.
  9. G. E. Stan et al., "Critical advances in the field of magnetron sputtered bioactive glass thin-films: An analytical review," Applied Surface Science, vol. 646, no. February, p. 158760, 2024/02/15/ 2024, doi: https://doi.org/10.1016/j.apsusc.2023.158760.
  10. K. Shahapurkar et al., "Comprehensive review on polymer composites as electromagnetic interference shielding materials," Polymers and Polymer Composites, vol. 30, no. 1, p. 09673911221102127, 2022, doi: https://doi.org/10.1177/09673911221102127.
  11. V. F. Nunes, P. H. F. Maia, A. F. L. Almeida, and F. N. A. Freire, "Surface properties of Al2O3:ZnO thin films growth on FTO for photovoltaic application," Next Materials, vol. 2, no. January, p. 100069, 2024/01/01/ 2024, doi: https://doi.org/10.1016/j.nxmate.2023.100069.
  12. J. M. Taha, R. A. Nassif, N. H. Numan, and M. A. Fakhri, "Effects of oxygen gas on the physical properties of tin oxide nano films using laser light as ablation source," AIP Conference Proceedings, vol. 2213, no. 1, p. 020235, 2020, doi: https://doi.org/10.1063/5.0000198.
  13. M. I. Ahmed, H. S. Jahin, H. A. Dessouki, and M. Y. Nassar, "Synthesis and characterization of γ-Al2O3 and α-Al2O3 nanoparticles using a facile, inexpensive auto-combustion approach," Egyptian Journal of Chemistry, vol. 64, no. 5, pp. 2509-2515, 2021, doi: https://doi.org/10.21608/ejchem.2021.61793.3330.
  14. P. S. Prevéy, "The measurement of subsurface residual stress and cold work distributions in nickel base alloys," in ASM’s conference on residual stress in design, process and materials selection, Cincinnati, Ohio, USA, W. B. Young, Ed., 1987: ASM International, pp. 11-20.
  15. R. A. Abeer, A. A. Ali, A. F. Makram, A. Q. Motahher, and C. B. G. Subash, "Optical properties of Al2O3 thin film deposited by pulsed laser deposition technique," International Journal of Nanoelectronics and Materials (IJNeaM), vol. 18, no. 2, pp. 256-262, 05/05 2025, doi: https://doi.org/10.58915/ijneam.v18i2.2124.
  16. H.-J. Kim and S.-M. Nam, "High loading of nanostructured ceramics in polymer composite thick films by aerosol deposition," Nanoscale Research Letters, vol. 7, no. 1, p. 92, 2012/01/27 2012, doi: https://doi.org/10.1186/1556-276X-7-92.
  17. S. Y. Lee, E. W. Huang, W. Woo, C. Yoon, H. Chae, and S.-G. Yoon, "Dynamic Strain Evolution around a Crack Tip under Steady- and Overloaded-Fatigue Conditions," Metals, vol. 5, no. 4, pp. 2109-2118doi: https://doi.org/10.3390/met5042109.
  18. M. A. Fakhri et al., "Effect of different laser wavelengths on the optical properties of GaN/PSi and Al2O3/PSi thin films using the pulse laser deposition method," Journal of Optics, vol. 53, no. 5, p. 02393, 2024/12/30 2024, doi: https://doi.org/10.1007/s12596-024-02393-w.
  19. N. E. Naji, A. A. Aljubouri, and R. A. Ismail, "Structural Characteristics of Alumina Nanoparticles Synthesised by DC Reactive Sputtering Technique," Journal of Applied Sciences and Nanotechnology, vol. 5, no. 3, pp. 13-23, 2025, doi: https://doi.org/10.53293/jasn.2025.7575.1335.
  20. E. Sivasenthil, R. Nandhini, D. Tamilselvi, and R. Raja, "Synthesis and characterization of Al2O3 nanoparticles by using co-precipitation method," AIP Conference Proceedings, vol. 2861, no. 1, p. 020008, 2023, doi: https://doi.org/10.1063/5.0160270.
  21. D. A. Mohammed, A. Kadhim, and M. A. Fakhri, "The enhancement of the corrosion protection of 304 stainless steel using Al2O3 films by PLD method," AIP Conference Proceedings, vol. 2045, no. 1, p. 020014, 2018, doi: https://doi.org/10.1063/1.5080827.